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The paper aims to investigate the effect of zinc dialkyldithiophosphate (ZDDP) on wear and extreme pressure (EP) capabilities of hazelnut oil.

A four-ball tribometer is used to study the effect of ZDDP on the antiwear (AW) and EP performance of hazelnut oil as a lubricant. The AW/EP tests are carried out following ASTM D4172 and ASTM D2783 standards. The wear mechanism of steel balls is studied by scanning electron microscope (SEM). The ZDDP is added in 1Wt.%, 2Wt.% and 3Wt.% concentration, and its presence on surfaces is indicated by Energy Dispersive X-Ray Analysis (EDX).

The maximum improvement in the wear properties for hazelnut oil is equal to 43.7% and 45.7% at 1Wt.% and 3Wt. % ZDDP, respectively. Also, the load wear index of hazelnut oil increases from 29 to 73.1 at 3Wt.% ZDDP. The improvement in AW and EP properties is attributed to the protective layer formation by ZDDP.

The paper is a novel study investigating the effect of ZDDP additive in hazelnut oil. The results could prove beneficial in making the hazelnut oil a viable replacement of mineral oils.

The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-06-2020-0217/

Formulation of mineral-based specialty lubricants without anti-wear (AW) and extreme-pressure (EP) additives is a challenging task. This study aims to propose an environment friendly alternative to mineral-based lubricants with superior wear preventive characteristics.

In this study, analysis of wear under trimethylolpropane trioleate (TMPTO)-based lube using operating parameters of four-ball tester was done. The effects of type of lube oil, temperature, load and speed on specific wear rate were investigated using Taguchi L27 orthogonal array. Based on the Taguchi experimental results and single-to-noise ratios, ranking of the four ball parameters was done. The surface analysis of worn steel balls was carried out using optical microscopic images of wear scar and energy dispersive spectrometry (EDS).

Results depict that the blend of sulfurized additives with TMPTO base oil showed a synergistic effect in terms of reduction in specific wear rate by the formation of protective film layer on the surface. The possible physical or chemical interactions between base oil and additives were studied based on the surface morphology of test balls.

The formulated lubricant has the potential to be used as a tapping/broaching oil.

To the best of the authors’ knowledge, the paper is a novel study investigating the effect of different additive in TMPTO. The results could prove beneficial in making TMPTO-based lube oil a viable replacement of mineral-based oils.

The purpose of this study is to investigate the tribological performance (anti-friction and anti-wear properties) of commercial Mobil grade lubricants used in a journal bearing system in a power plant.

Three grades of Mobil lubricants (DTE 24, DTE 25 and DTE 26) are considered during the study. Titanium dioxide nanoparticles (TiO₂, 0.5 Wt.%) of size 40 nm are used as a lubricant additive to examine the performance of the lubricants. The viscosity of the lubricant is computed using modified Krieger–Dougherty viscosity model. The morphology of TiO₂ nanoparticles is studied with the help of scanning electron microscopy, ultra violet spectrophotometer and X-ray diffraction. The study of antifriction and antiwear properties for lubricants is carried out on four-ball tribo-tester for operating conditions specified by ASTM standards.

The tribochemical reaction film is formed between ball surfaces during the experiments on four-ball tester that minimizes the asperity contact due to addition of TiO₂ nanoparticles in the lubricant. The viscosity of the lubricant is enhanced due to the addition of TiO₂ nanoparticles. The frictional coefficient and wear scar diameters of balls in the lubricants are reduced in the range of 6-26 and 2-7 per cent, respectively.

The tribological properties of TiO₂ as a lubricant additive in three commercial Mobil grade lubricants are investigated in this paper. The results obtained in this paper are expected to be helpful to bearing designers, researchers and academicians concerned with the relevant study.

The screening of lube oil performance prior to field trials is the most significant for the formulation of novel lubricants. This paper aims to investigate the efficacy of trimethylolpropane trioleate oil (TMPTO) based lubricants with different additives.

In this endeavor, initially five lubricating blends along-with TMPTO based oil with variable additives were evaluated for their tribological performances using ASTM standards. Out of these, the top three best-performing oils were further investigated for possible physical or chemical synergies among lube oils, additives and ball surface using SEM. The molecule structures of TMPTO based lube oils were confirmed using Fourier transform infrared spectroscopy (FTIR).

The wear preventive and extreme pressure characteristics of different TMPTO based samples were evaluated and compared for compatibility and synergy of additives. Morphological analysis of SEM images was used to understand the wear behavior of the worn surfaces.

Further investigation of TMPTO oil on its oxidation stability at high temperature and pressure to make it technologically competitive and commercially viable metal-working lubricant is suggested.

This paper highlights the tribo-effects of TMPTO to be rendered as a suitable lubricant for metal-cutting operations. The surface morphology of the worn-out surface significantly demonstrates the effect of loading conditions.

This study aims to investigate the behavior of vegetable oil with two additives. Base oil’s tribological qualities can be improved with the help of several additions. In the present investigation, soybean oil is served as the foundational oil due to its eco-friendliness and status as a vegetable oil with two additives, named polytetrafluoroethylene (PTFE) and molybdenum disulfide (MoS₂).

As additives, PTFE and MoS₂ are used; PTFE is renowned for its anti-friction (AF) properties, while MoS₂ is a solid lubricant with anti-wear (AW) properties. This investigation examines the synergistic impact of AF and AW additions in vegetable oil. The lubricity of the base oil is measured by using a four-ball tester, and the wear properties of the oil at different additive amounts are determined by using a universal tribometer.

PTFE (at 5 Wt.%) and MoS₂ (at 1 Wt.%) were found to improve the tribological performance of the base oil. The weld load is significantly increased when 5 Wt.% of PTFE + MoS₂ is added to the base oil.

A better tribological characteristic can be achieved by combining additives that amount to less than 1% of the base oil. In experiments with highly concentrated MoS₂, the adequate pressure improved dramatically, but the lubricant’s tribological characteristics did not.

The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-11-2022-0321/

The purpose of this study is to reduce the use of Zinc dialkyl dithiophosphates (ZDDP) and improve the frictional properties and thermal oxidation stability of Perfluoropolyether (PFPE) grease by adding antioxidant additives. The addition of antioxidants can reduce the consumption of ZDDP as an antioxidant, thus improving the anti-wear efficiency of ZDDP and reducing the excess phosphorus element in the grease.

In this study, an antioxidant with good comprehensive performance was selected from several antioxidants by tribological tests and high-temperature tests. Then, the effect of its combination additive with ZDDP on PFPE grease was investigated. The anti-wear property, anti-friction property, thermal oxidation stability and extreme pressure property of greases containing different proportions of ZDDP and antioxidant were tested by four-ball tester and synchronous thermal analyzer (STA). The effects of additives on properties of grease were analyzed by SEM, EDS, LSCM, XPS and FT-IR.

The research shows that 2,6-Di-tert-butyl-4-methylphenol (BHT) can be used as an antioxidant in combined additives to reduce the antioxidant reactions of ZDDP, thus improving the anti-wear efficiency of ZDDP and further enhancing the anti-wear performance of the grease. Moreover, BHT and ZDDP have a synergistic effect on the high temperature performance of the PFPE grease due to their different antioxidant mechanisms.

In this paper, the problems related to PFPE grease are studied, which has a certain guiding effect on the industrial application of fluorine grease and the related formulation design.

In this paper, the properties of PFPE grease under different lubricating condition were studied. The synergistic lubrication effect of antioxidant and ZDDP are discussed. It provides experimental and theoretical support for reducing the content of ZDDP and improving the performance of additives.

This paper aims to investigate the tribological properties of two protic ionic liquids used as lubricity-improving additives in the water. Their concentration was optimized for different metal friction pairs including bearing steel, stainless steel and aluminum alloy.

In this study tribological properties were investigated by using a ball-on-plate reciprocating tribometer. Three different friction pairs were selected: bearing steel-bearing steel; bearing steel-stainless steel; bearing steel-aluminum alloy. To optimize the concentration of investigated protic ionic liquids four concentrations were selected. Wettability was investigated using the droplet method. The corrosiveness of additive-loaded water was investigated using the iron chip method.

The results show that by using protic ionic liquids the lubricity of water could be greatly improved. However, the friction pair material and additive concentration play a significant role. The positive tribological effect was attributed to the polarity of the additive molecule which tends to form an adsorption layer. The polarity of molecules also leads to better surface wettability. It was also found that both investigated protic ionic liquids can improve the anticorrosion properties of water.

To the best of the authors’ knowledge, this is the first study to present a complex investigation of tribological properties of two protic ionic liquids as additives in the water. In this case, three different metal friction pairs and four additive concentrations were investigated. The results could be interesting to those who are working in the field of water-based lubricants and luck for multipurpose lubricity-improving additives.

The involvement of wear, friction and lubrication in engineering systems and industrial applications makes it imperative to study the various aspects of tribology in relation with advanced technologies and concepts. The concept of Industry 4.0 and its implementation further faces a lot of barriers, particularly in developing economies. Real-time and reliable data is an important enabler for the implementation of the concept of Industry 4.0. For availability of reliable and real-time data about various tribological systems is crucial in applying the various concepts of Industry 4.0. This paper aims to attempt to highlight the role of sensors related to friction, wear and lubrication in implementing Industry 4.0 in various tribology-related industries and equipment.

A through literature review has been done to study the interrelationships between the availability of tribology-related data and implementation of Industry 4.0 are also discussed. Relevant and recent research papers from prominent databases have been included. A detailed overview about the various types of sensors used in generating tribological data is also presented. Some studies related to the application of machine learning and artificial intelligence (AI) are also included in the paper. A discussion on fault diagnosis and cyber physical systems in connection with tribology has also been included.

Industry 4.0 and tribology are interconnected through various means and the various pillars of Industry 4.0 such as big data, AI can effectively be implemented in various tribological systems. Data is an important parameter in the effective application of concepts of Industry 4.0 in the tribological environment. Sensors have a vital role to play in the implementation of Industry 4.0 in tribological systems. Determining the machine health, carrying out maintenance in off-shore and remote mechanical systems is possible by applying online-real-time data acquisition.

The paper tries to relate the pillars of Industry 4.0 with various aspects of tribology. The paper is a first of its kind wherein the interdisciplinary field of tribology has been linked with Industry 4.0. The paper also highlights the role of sensors in generating tribological data related to the critical parameters, such as wear rate, coefficient of friction, surface roughness which is critical in implementing the various pillars of Industry 4.0.

Studies on this topic have shown the remarkable lubricating properties, viz. friction-reducing and anti-wear, of certain nanoparticles. This makes them potential candidates for replacing the lubrication additives currently used in automobile lubricants, especially because the latter is known to be pollutants and less efficient in some specific conditions. This has not gone unnoticed to professionals in the sector, including those commercializing these additives, the oil companies and the car industry, all of whom are following this burgeoning research area with keen interest. All of them are faced with the problem of providing lubricants that meet the needs of the technological evolution of engines while respecting ever-stricter environmental norms.

The impact of copper oxide (CuO) and zinc oxide (ZnO) nanoparticles on the tribological properties of the SAE-40 pure diesel oil is studied in this paper. The two nanoparticles are not oxide or deteriorate with the base oil. The average size of CuO and ZnO nanoparticles is 40 and 20 nm, respectively. Nanoparticle concentrations of 0.1 Wt.%, 0.2 Wt.%, 0.3 Wt.%, 0.4 Wt.% and 0.5 Wt.% are tested using a pin-on-disk tribometer to evaluate their impact on friction and wear. The test is carried out at different loads and rotating speeds of 58.86 N and 300 rpm, 39.24 N and 500 rpm and 78.48 N and 900 rpm at room temperature, respectively.

The obtained results of the nanolubricants are compared with those of pure diesel oil in terms of % improvement in tribological properties. However, it is observed that an increase in the nanoparticle concentrations does not guarantee to enhance the tribological properties. Similarly, increasing the applied load and the rotating speed does not lead to improving the anti-friction and anti-wear properties. The results obtained revealed that the optimal improvements in the anti-friction and anti-wear properties of the pure oil are 69% and 77% when CuO nanoparticle concentrations of 0.3 Wt.% and the ZnO nanoparticle concentrations of 0.1 Wt.% are used, where the applied load and rotating speed are 39.24 N and 500 rpm, respectively. It has also been noticed that the CuO nanolubricants have a significant impact on the anti-friction property compared with ZnO nanolubricants.

All these nanoparticles have been the subject of detailed investigation in this research and many key issues have been tackled, such as the conditions leading to these properties, the lubrication mechanisms coming into play, the influence of parameters such as size, structure and morphology of the nanoparticles on their tribological properties/lubrication mechanisms and the interactions between the particles and the lubricant co-additives. To answer such questions, state-of-the-art characterization techniques are required, often in situ, and sometimes an extremely complex set up. Some of these can even visualize the behavior of a nanoparticle in real time during a tribological test. The research on this topic has given a good understanding of the way these nanoparticles behave, and we can now identify the key parameters to be adjusted when optimizing their lubrication properties.

The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-08-2022-0234/

The purpose of this study is to investigate the mechanical and tribological properties of the synthetic diamond coatings deposited on WC-Co cutting tools for their prospective applications in mechanical industry. In this work, the concept of nanocrystalline diamond, microcrystalline diamond and multilayer-diamond coating systems were proposed and deposited on WC-Co substrates with the top-layer nanocrystallinity, optimum thickness and interfacial adhesion strength for load-bearing tribological and machining applications. Also, the overall mechanical and tribological properties of all synthetic diamond coatings were compared for the purpose of selecting a suitable type of protective layer used on the surfaces of WC-Co cutting tools or mechanical dies.

Smooth and adhesive single layered and multilayered synthetic deposited on chemically etched cemented tungsten carbide (WC-Co) substrates using predetermined process parameters in hot filament chemical vapor deposition (HFCVD) method. A comparison has been documented between diamond coatings having different nature and architecture for the purpose of studying their mechanical and tribological characteristics. The friction characteristics were studied experimentally using ball-on-disc type linear reciprocating micro-tribometer under the influence of varying load conditions and within dry sliding conditions. Nanoindentation tests were conducted on each diamond coating using Berkovich nanoindenter for the measurement of their hardness and elastic modulus values. Also, the wear characteristics of all sliding bodies were studied under varying load conditions using cumulative weight loss and density method.

Depositing any type of diamond coating on the cemented carbide tool insert increases its all mechanical and tribological characteristics. When using boron-doping onto the top-layer surface of diamond coatings decrease slightly their mechanical properties but increases the tribological characteristics. Present analysis reveals that friction coefficient of all diamond-coated WC-Co substrates decreases with the increase of normal load. Therefore, maintaining an appropriate level of normal load, sliding time, sliding distance, atmospheric conditions and type of diamond coating, the friction coefficient may be kept to some lower value to improve mechanical processes.

As the single layered synthetic diamond coatings have not given the full requirements of mechanical and tribological properties when deposited on cutting tools. Therefore, the multilayered diamond coatings were proposed and developed to enhance the interfacial integrity of the nanocrystalline and microcrystalline layers (by eliminating the sharp interface) as well as increasing the hardness of tungsten carbide substrate. However, when using boron doping onto the top-layer surface of diamond, coatings decreases slightly their mechanical characteristics but also decreases the value of friction coefficient.